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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1281828Generated: October 31, 2026

1,1-Ethanedithiol → HCID 135816412, compound

https://huagongshe.com/reaction/1281828

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,1-EthanedithiolHCID 33645—
ReactantAluminum(III) ChlorideHCID 6451240—
ReactantHCID 135816423HCID 135816423—
SolventDichloromethaneHCID 6344—
ProductHCID 135816412HCID 135816412—

Reaction Steps

In the same manner as in Example 62 and using 8-fluoro-9-methoxy-12-(4-methylpiperazin-1-yl)-6H-[1]benzothieno[2,3-b][1,5]benzodiazepine, dichloromethane, ethanedithiol and aluminium chloride, 8-fluoro-9-hydroxy-12-(4-methylpiperazin-1-yl)-6H-[1]benzothieno[2,3-b][1,5]benzodiazepine is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06455521B1
Source datasetuspto-grants-2002_09
ORD IDord-749cfec88e324bb4b3ea47952d26e7f9
Source noteuspto-grants-2002_09