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Thionyl Chloride → N-(4-fluoro-2-hydroxyphenyl)-2-bromo-5-methyl-3-thiophenecarboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 2-Amino-5-fluorophenol | HCID 185763 | — |
| 反応物 | 2-Bromo-5-methylthiophene-3-carboxylic acid | HCID 11117589 | — |
| 生成物 | N-(4-fluoro-2-hydroxyphenyl)-2-bromo-5-methyl-3-thiophenecarboxamide | HCID 18422331 | — |
反応手順
In the same manner as in Starting Material Synthesis Example 67 and using 2-bromo-5-methyl-3-thiophenecarboxylic acid, thionyl chloride and 2-amino-5-fluorophenol, N-(4-fluoro-2-hydroxyphenyl)-2-bromo-5-methyl-3-thiophenecarboxamide is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06455521B1 |
| 出典データセット | uspto-grants-2002_09 |
| ORD ID | ord-4c511034c7234e9e90ca7860fec0d683 |
| 出典メモ | uspto-grants-2002_09 |