HCID 18423492, compound → HCID 18423421, compound

Participants

Reaction Steps

A mixture of 0.09 g (0.3 mmol) of 1-t-butoxycarbonyl-4-(2-allyloxy-2-methyl-1-propyl)piperidine and 0.0058 g of Pd/C (10%) in 2 mL of CH3OH was stirred under H2 (1 atm) for 24 h. The reaction mixture was filtered through a thin pad of Celite and the filtrate was concentrated. The residue was purified by chromatography (silica, hexanes:ether, 6:1) to give 0.06 g of the title compound.

Provenance & Evidence