HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Formyl-6-methoxyphenoxy)acetaldehyde → 7-Methoxy-1-benzofuran-2-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Formyl-6-methoxyphenoxy)acetaldehyde | HCID 18423653 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 7-Methoxy-1-benzofuran-2-carbaldehyde | HCID 3457310 | — |
Reaction Steps
2-(2-Formyl-6-methoxyphenoxy)acetaldehyde, dimethyl acetal (31 g) was heated to reflux in glacial acetic acid (120 ml) overnight. The mixture was then cooled and the solvent removed in vacuo to give a red oil. Purification by Kugelrohr distillation gave the title compound (17 g) as a pale yellow oil which solidified on standing.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455561B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-0c11d8ce34964ba38139aaa086af1edc |
| Source note | uspto-grants-2002_09 |