HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Amino-3,5-dimethylisoxazole → HCID 10155190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Amino-3,5-dimethylisoxazole | HCID 182040 | — |
| Reactant | HCID 18423650 | HCID 18423650 | — |
| Product | HCID 10155190 | HCID 10155190 | 66.8% |
Reaction Steps
Starting from 7-methoxy-2-(tetrahydrofuran-2-yl)-benzofuran-4-carboxylic acid (262 mg) and 3,5-dimethylisoxazol-4-ylamine (120 mg). Purification by column chromatography on silica eluting with 30% ethyl acetate in hexane afforded the title compound as an off-white solid (238 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455561B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-7cf4d592544b4ca9bd15c58831aff9e5 |
| Source note | uspto-grants-2002_09 |