反应详情

Into a three-necked 500 ml round-bottom flask are charged 25 g (0.125 mole) of o-phenoxy benzyl alcohol and 200 ml of benzene. To this solution is added 18 g (0.15 mole) of thionyl chloride dropwise with stirring. The reaction mixture is then heated to reflux for four hours. Solvent and excess thionyl chloride are removed under vacuum to give 30 g of product.

1. temperatureThe reaction mixture is then heated
2. temperatureto reflux for four hours
3. customSolvent and excess thionyl chloride are removed under vacuum