HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-methylphenyl isothiocyanate → HCID 9947534, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-methylphenyl isothiocyanate | HCID 29519 | — |
| Reactant | 4-Thiazoleacetic acid, 2-amino-, ethyl ester | HCID 104454 | — |
| Product | HCID 9947534 | HCID 9947534 | 40% |
Reaction Steps
Prepared using Method B from 4.5 g (24.5 mmol) of 5-chloro-2-methyl-phenyl isothiocyanate and 4.56 g (24.5 mmol) of 2-(2-amino-thiazol-4-yl)-acetic acid ethyl ester to give 3.62 g of title compound as a white solid (40% yield, m.p. 177-179° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455566B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-98e0b73990ca4698ada42803468d136a |
| Source note | uspto-grants-2002_09 |