HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → Bis-(1H-imidazol-2-YL)-methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Product | Bis-(1H-imidazol-2-YL)-methanone | HCID 5250894 | — |
| Product | Imidazolium chloride | HCID 10197644 | — |
Reaction Steps
Reaction of imidazole with bis (trichloromethyl) carbonate produces carbonyl diimidazole and crystalline imidazole hydrochloride. Insoluble imidazole hydrochloride is removed from the reaction mixture quantitatively by filtration and the carbonyl diimidazole is recovered by removing the solvent or crystallization under cooling or a combination thereof.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455702B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-f734730a142b45d28a7983dd411b3709 |
| Source note | uspto-grants-2002_09 |