HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Aurone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3-Carboxybenzaldehyde | HCID 12077 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Product | Aurone | HCID 6537099 | — |
Reaction Steps
This product was immediately dissolved in dioxane (50 ml.), 3-carboxybenzaldehyde (4.5 g., 0.03 mole) added, followed by concentrated hydrochloric acid (10 ml) and the solution heated on a steam bath for 15 minutes. Work up was as Example 49 with recrystallisation from dimethylformamide to give the desired aurone, m.p. 280° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04259340 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-e9c909ec3ac1422ea0bb4da643dfa9b8 |
| Source note | uspto-grants-1981_03 |