2-Propenoic acid, 3-(3-nitrophenyl)- → HCID 86604348, compound

HRID 1282518Notes

Reaction equation

HRID 1282518 reaction equation
[CH2:1]([N:5]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[C@H:6]([C:12]([OH:14])=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][NH2:11])[CH:2]([CH3:4])[CH3:3].[N+:27]([C:30]1[CH:31]=[C:32]([CH:38]=[CH:39][CH:40]=1)[CH:33]=[CH:34][C:35](O)=[O:36])([O-:29])=[O:28]>>[CH2:1]([N:5]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[C@H:6]([C:12]([OH:14])=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][NH:11][C:35](=[O:36])[CH:34]=[CH:33][C:32]1[CH:38]=[CH:39][CH:40]=[C:30]([N+:27]([O-:29])=[O:28])[CH:31]=1)[CH:2]([CH3:4])[CH3:3]

Participants

3

Reactant 2

HCID 683902-Propenoic acid, 3-(3-nitrophenyl)-HCID 69107391HCID 69107391, compound

Product 1

HCID 86604348HCID 86604348, compoundYield 52%

Procedure

Nα-isobutyl-Nα-(4-nitrobenzenesulfonyl)-L-lysine was reacted with 3-nitrocinnamic acid under the conditions described in example 86 to yield 52% of the desired product.

Sources & evidence

ORD record
ord-3136da1c030e41e68e350e9430296536
Source dataset
uspto-grants-2002_09
Patent number
US06455587B1

Reaction notes

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