3-(2,4-Dimethoxyphenyl)prop-2-enoic acid → HCID 86604352, compound

HRID 1282523Notes

Reaction equation

HRID 1282523 reaction equation
[CH2:1]([N:5]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[C@H:6]([C:12]([OH:14])=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][NH2:11])[CH:2]([CH3:4])[CH3:3].[CH3:27][O:28][C:29]1[CH:39]=[C:38]([O:40][CH3:41])[CH:37]=[CH:36][C:30]=1[CH:31]=[CH:32][C:33](O)=[O:34]>>[CH2:1]([N:5]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[C@H:6]([C:12]([OH:14])=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][NH:11][C:33](=[O:34])[CH:32]=[CH:31][C:30]1[CH:36]=[CH:37][C:38]([O:40][CH3:41])=[CH:39][C:29]=1[O:28][CH3:27])[CH:2]([CH3:4])[CH3:3]

Participants

3

Reactant 2

HCID 856363-(2,4-Dimethoxyphenyl)prop-2-enoic acidHCID 69107391HCID 69107391, compound

Product 1

HCID 86604352HCID 86604352, compoundYield 72%

Procedure

Nα-isobutyl-Nα-(4-nitrobenzenesulfonyl)-L-lysine was reacted with 2,4-dimethoxycinnamic acid under the conditions described in example 86 to yield 72% of the desired product.

Sources & evidence

ORD record
ord-a010184a80224be28e75ce5550454ce3
Source dataset
uspto-grants-2002_09
Patent number
US06455587B1

Reaction notes

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