2-Propenoic acid, 3-(4-nitrophenyl)- → HCID 86604353, compound

HRID 1282524Notes

Reaction equation

HRID 1282524 reaction equation
[CH2:1]([N:5]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[C@H:6]([C:12]([OH:14])=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][NH2:11])[CH:2]([CH3:4])[CH3:3].[N+:27]([C:30]1[CH:40]=[CH:39][C:33]([CH:34]=[CH:35][C:36](O)=[O:37])=[CH:32][CH:31]=1)([O-:29])=[O:28]>>[CH2:1]([N:5]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[C@H:6]([C:12]([OH:14])=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][NH:11][C:36](=[O:37])[CH:35]=[CH:34][C:33]1[CH:32]=[CH:31][C:30]([N+:27]([O-:29])=[O:28])=[CH:40][CH:39]=1)[CH:2]([CH3:4])[CH3:3]

Participants

3

Reactant 2

HCID 701562-Propenoic acid, 3-(4-nitrophenyl)-HCID 69107391HCID 69107391, compound

Product 1

HCID 86604353HCID 86604353, compoundYield 49%

Procedure

Nα-isobutyl-Nα-(4-nitrobenzenesulfonyl)-L-lysine was reacted with 4-nitrocinnamic acid under the conditions described in example 86 to yield 49% of the desired product.

Sources & evidence

ORD record
ord-b40d44f8e4d04472b10a2559a41189da
Source dataset
uspto-grants-2002_09
Patent number
US06455587B1

Reaction notes

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