4-Methoxy cinnamic acid → HCID 86604354, compound

HRID 1282525Notes

Reaction equation

HRID 1282525 reaction equation
[CH2:1]([N:5]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[C@H:6]([C:12]([OH:14])=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][NH2:11])[CH:2]([CH3:4])[CH3:3].[CH3:27][O:28][C:29]1[CH:39]=[CH:38][C:32]([CH:33]=[CH:34][C:35](O)=[O:36])=[CH:31][CH:30]=1>>[CH2:1]([N:5]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[C@H:6]([C:12]([OH:14])=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][NH:11][C:35](=[O:36])[CH:34]=[CH:33][C:32]1[CH:38]=[CH:39][C:29]([O:28][CH3:27])=[CH:30][CH:31]=1)[CH:2]([CH3:4])[CH3:3]

Participants

3

Reactant 2

HCID 132454-Methoxy cinnamic acidHCID 69107391HCID 69107391, compound

Product 1

HCID 86604354HCID 86604354, compoundYield 65%

Procedure

Nα-isobutyl-Nα-(4-nitrobenzenesulfonyl)-L-lysine was reacted with 4-methoxycinnamic acid under the conditions described in example 86 to yield 65% of the desired product.

Sources & evidence

ORD record
ord-61f4b4605543453298b2be8ca99aeaed
Source dataset
uspto-grants-2002_09
Patent number
US06455587B1

Reaction notes

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