P-Coumaric Acid → HCID 86604362, compound

HRID 1282532Notes

Reaction equation

HRID 1282532 reaction equation
[CH2:1]([N:5]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[C@H:6]([C:12]([OH:14])=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][NH2:11])[CH:2]([CH3:4])[CH3:3].[OH:25][C:26]1[CH:36]=[CH:35][C:29](/[CH:30]=[CH:31]/[C:32](O)=[O:33])=[CH:28][CH:27]=1>>[CH2:1]([N:5]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[C@H:6]([C:12]([OH:14])=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][NH:11][C:32](=[O:33])/[CH:31]=[CH:30]/[C:29]1[CH:35]=[CH:36][C:26]([OH:25])=[CH:27][CH:28]=1)[CH:2]([CH3:3])[CH3:4]

Participants

3

Reactant 2

HCID 637542P-Coumaric AcidHCID 23552860Nalpha-isobutyl-Nalpha-(4-methylbenzenesulfonyl)-L-lysine

Product 1

HCID 86604362HCID 86604362, compoundYield 45%

Procedure

Nα-isobutyl-Nα-(4-methylbenzenesulfonyl)-L-lysine was reacted with trans-4-hydroxycinnamic acid under the conditions described in example 86 to yield 45% of the desired product.

Sources & evidence

ORD record
ord-46ecef95ac694fbd84d736c5e1458fb0
Source dataset
uspto-grants-2002_09
Patent number
US06455587B1

Reaction notes

Loading…