HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 12462519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 2-Imidazolidinone | HCID 8453 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 12462519 | HCID 12462519 | — |
Reaction Steps
86 parts by weight of 2-oxo-imidazolidine, 194 parts by weight of benzenesulphonyl chloride, 800 parts by volume of tetrahydrofurane, 500 parts by volume of chloroform and 101 parts by weight of triethylamine were stirred overnight at 50°C and subsequently evaporated to dryness in vacuo. The residue was gradually added, while stirring, to 1,000 parts by volume of ice water, the mixture was filtered and the residue was recrystallized from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03972870 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-5bdc4a47fc5c4a6eb25b602d8f65289a |
| Source note | uspto-grants-1976_08 |