HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 12771221, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 2-Oxoimidazolidine-1-carbonyl chloride | HCID 83241 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 12771221 | HCID 12771221 | — |
Reaction Steps
14.9 parts by weight of N-chlorocarbonylimidazolid-2-one in 100 parts by volume of i-propanol and 100 parts by volume of dioxane were warmed to 50° C for 3 hours. After stripping off the solvent, the residue was recrystallized from acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03972869 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-7b7195bafe884708b9fcfc0415aba76a |
| Source note | uspto-grants-1976_08 |