HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → HCID 13031822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 2(1H)-Pyrimidinone, tetrahydro- | HCID 74615 | — |
| Product | HCID 13031822 | HCID 13031822 | — |
Reaction Steps
This compound was produced as described in Example 35 C from 10 parts by weight of 1,3-diaza-cyclohexan-2-one, 49 parts by weight of trimethylchlorosilane and 30 parts by weight of mesylchloride. The reaction product was recrystallized from acetone at low temperature and thereafter from acetone/ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03972869 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-203be615736147cea11e6bfd105c7184 |
| Source note | uspto-grants-1976_08 |