HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzaldehyde → 1-Nitro-4-((E)-styryl)-benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzaldehyde | HCID 541 | — |
| Catalyst | Benzyltriphenylphosphonium chloride | HCID 70671 | — |
| Product | 1-Nitro-4-((E)-styryl)-benzene | HCID 98001 | — |
Reaction Steps
Using the procedure of Example 5 benzyltriphenylphosphonium chloride (0.1 mole) and 4-nitrobenzaldehyde (0.1 mole) are reacted to give 4-nitrostilbene. The 4-nitrostilbene is reduced with palladium on charcoal as the catalyst to 4-(2'-phenethyl)aniline, m.p. 46°-50° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03972926 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-344ce71790de4d70827b7395c0f21780 |
| Source note | uspto-grants-1976_08 |