HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrobenzaldehyde → HCID 285594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrobenzaldehyde | HCID 7449 | — |
| Catalyst | Benzyltriphenylphosphonium chloride | HCID 70671 | — |
| Product | HCID 285594 | HCID 285594 | — |
Reaction Steps
Using the procedure of Example 5 benzyltriphenylphosphonium chloride and 3-nitrobenzaldehyde are reacted to give 3-nitrostilbene which is selected to 3-aminostilbene. The 3-aminostilbene is sulfonylated to give 3-(2'-phenethyl)trifluoromethanesulfonanilide, m.p. 64.5°-66° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03972926 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-14aae489078845b69d59ae8778a91086 |
| Source note | uspto-grants-1976_08 |