Octylamine → N-n-octyl-3,5-di-t-butyl-4-hydroxybenzamide

HRID 1282877Notes

Reaction equation

[CH2:1]([NH2:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[C:10]([C:14]1[CH:15]=[C:16]([CH:20]=[C:21]([C:24]([CH3:27])([CH3:26])[CH3:25])[C:22]=1[OH:23])[C:17](Cl)=[O:18])([CH3:13])([CH3:12])[CH3:11]>>[CH2:1]([NH:9][C:17](=[O:18])[C:16]1[CH:20]=[C:21]([C:24]([CH3:25])([CH3:26])[CH3:27])[C:22]([OH:23])=[C:14]([C:10]([CH3:13])([CH3:12])[CH3:11])[CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

Reactant 2

HCID 8143Octylamine

HCID 37871873,5-Di-tert-butyl-4-hydroxybenzoyl chloride

Product 1

HCID 21564370N-n-octyl-3,5-di-t-butyl-4-hydroxybenzamide

Procedure

In the manner of Example 1, n-octylamine was reacted with 3,5-di-t-butyl-4hydroxybenzoyl chloride to produce N-n-octyl-3,5-di-t-butyl-4-hydroxybenzamide; melting point 133°-135°C. When tested by the procedure of Example 2, the sample containing this compound lasted 1000 hours, about 3.3 times as long as the control.

Sources & evidence

ORD record: ord-b60cb056bb2c4100acde121bfe79a843
Source dataset: uspto-grants-1976_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03972927

Reaction notes

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