HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 178455938, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 178455937 | HCID 178455937 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178455938 | HCID 178455938 | — |
Reaction Steps
Pyroglutamyl-tryptophyl-prolyl-arginyl-prolyl-glutaminyl-isoleucyl-prolyl-proline (1.6 g) is dissolved in 80 ml of methanol. To this, excess ethereal diazomethane is added and the solution is kept for 7 hours at room temperature. Acetic acid is added to destroy the excess diazomethane and the resulting mixture is concentrated to dryness in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03973006 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-d833ec88638c453b8f1063f7b161eed8 |
| Source note | uspto-grants-1976_08 |