Ammonia → HCID 21499787, compound

HRID 1282972Notes

Reaction equation

HRID 1282972 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:13](=[O:14])[N:12]=[C:11]([O:15][CH3:16])[NH:10][C:9]2=[O:17])=[CH:4][CH:3]=1.[NH3:18]>CO>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([N:8]2[C:9](=[O:17])[N:10]=[C:11]([O:15][CH3:16])[NH:12][C:13]2=[O:14])=[CH:6][CH:7]=1.[NH4+:18]

Participants

4

Reactant 2

HCID 222AmmoniaHCID 186733AC1L4JFO

Product 1

HCID 21499787HCID 21499787, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

To a mixture of 10 parts of 3-(p-chlorophenyl)-6-methoxy-s-triazine-2,4(1H,3H)-dione and 100 parts of methanol is added 1 part of ammonia gas at 20°C. The solution is stirred for 30 minutes and then evaporated under vaccum to give 10.6 parts of ammonium 3-(p-chlorophenyl)-6-methoxy-s-triazine-2,4(1H,3H)-dione.

Workup

  1. customevaporated under vaccum

Sources & evidence

ORD record
ord-65cd643179f3499092f4eaebb4f113fa
Source dataset
uspto-grants-1976_08
Patent number
US03973947

Reaction notes

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