Phosgene → HCID 21453120, compound

HRID 1283034Notes

Reaction equation

HRID 1283034 reaction equation
[C:1]([Cl:4])(=[O:3])[NH2:2].[C:5]1([S:11]([N:14]2[CH2:19][CH2:18][CH2:17]N[C:15]2=[O:20])(=[O:13])=[O:12])[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.C(Cl)(Cl)=O>>[Cl:4][C:1]([N:2]1[CH2:17][CH2:18][CH2:19][N:14]([S:11]([C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][CH:10]=2)(=[O:13])=[O:12])[C:15]1=[O:20])=[O:3]

Participants

4

Reactant 3

HCID 6371PhosgeneHCID 68048Carbamic chlorideHCID 12462523HCID 12462523, compound

Product 1

HCID 21453120HCID 21453120, compound

Procedure

This carbamic acid chloride was produced as described in Example 27 A from 6 parts by weight of 1-phenylsulfonyl-1,3-diaza-cyclohexane-2-one and 5 parts by weight of phosgene. The product was recrystallized from acetone/petrolether.

Workup

  1. customThe product was recrystallized from acetone/petrolether

Sources & evidence

ORD record
ord-dd07f07c419e4f3d9bb5aac0ed663b10
Source dataset
uspto-grants-1976_08
Patent number
US03974141

Reaction notes

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