HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenol → omega-(4-Fluorophenoxy)-p-methylacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenol | HCID 9732 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Chloro-1-(4-methylphenyl)ethan-1-one | HCID 237805 | — |
| Product | omega-(4-Fluorophenoxy)-p-methylacetophenone | HCID 14970240 | — |
Reaction Steps
Following the procedure outlined in Example 11(a), 4-fluorophenol was interacted with an equimolar quantity of p-methylphenacyl chloride in the presence of potassium carbonate to give ω-(4-fluorophenoxy)-p-methylacetophenone which melted at 95°-96°C after recrystallization from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03974144 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-9cc5ce60d54c43aebea47becf4fba3ea |
| Source note | uspto-grants-1976_08 |