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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1283074Generated: October 31, 2026

4-Formylbenzoic acid → HCID 54439766, compound

https://huagongshe.com/reaction/1283074

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Formylbenzoic acidHCID 12088—
ReactantHCID 12659165HCID 12659165—
ReactantPotassium tert-butoxideHCID 23665647—
SolventDimethylformamideHCID 6228—
ProductHCID 54439766HCID 54439766—

Reaction Steps

Proceeding in a manner similar to that used in Example 1, 5-methyl-2-(p-tolyl)benzofuran (2.22 g; 0.01 mole) was interacted with 2.25 g (0.01 mole) of the anil derivative of terephthalaldehydic acid in the presence of 6.72 g (0.06 mole) of potassium tert-butoxide in 150 ml of dimethylformamide. The product thus produced was sublimed to obtain 5-methyl-2-[4-(4-carboxystyryl)phenyl ]benzofuran, melting at 355°-358°C. The wavelength of maximum excitation of this compound was 374 nm and the wavelength of maximum emission was 437 nm.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS03974144
Source datasetuspto-grants-1976_08
ORD IDord-b41550466c8b4ac69f196a5ff5a05cbb
Source noteuspto-grants-1976_08