HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Formylbenzoic acid → HCID 54439766, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Formylbenzoic acid | HCID 12088 | — |
| Reactant | HCID 12659165 | HCID 12659165 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54439766 | HCID 54439766 | — |
Reaction Steps
Proceeding in a manner similar to that used in Example 1, 5-methyl-2-(p-tolyl)benzofuran (2.22 g; 0.01 mole) was interacted with 2.25 g (0.01 mole) of the anil derivative of terephthalaldehydic acid in the presence of 6.72 g (0.06 mole) of potassium tert-butoxide in 150 ml of dimethylformamide. The product thus produced was sublimed to obtain 5-methyl-2-[4-(4-carboxystyryl)phenyl ]benzofuran, melting at 355°-358°C. The wavelength of maximum excitation of this compound was 374 nm and the wavelength of maximum emission was 437 nm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03974144 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-b41550466c8b4ac69f196a5ff5a05cbb |
| Source note | uspto-grants-1976_08 |