HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl chloroformate → HCID 86733813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | N-Phenyl-4-(phenylmethyl)-2-morpholinemethanamine | HCID 21430371 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86733813 | HCID 86733813 | — |
Reaction Steps
To a solution of 4-benzyl-2-anilinomethylmorpholine (8.1 g.) in toluene (50 ml.) and hexamethylene phosphoramide (2 ml.) is added phenylchloroformate (8 ml.). A white precipitate forms which does not dissolve when the mixture is refluxed for 4 hours. The solid (10.15 g.) is crystallised from ethanol to give 4-benzyl-2-(N-phenoxycarbonylanilino)methylmorpholine hydrochloride, m.p. 248°-250°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03974158 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-d8888cfa7af246e193f82156c7632e9a |
| Source note | uspto-grants-1976_08 |