HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanethiol → HCID 21519568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanethiol | HCID 878 | — |
| Reactant | 4,7,7-Trimethylbicyclo[4.1.0]hept-3-en-2-one | HCID 13502875 | — |
| Product | HCID 21519568 | HCID 21519568 | — |
Reaction Steps
In accordance with the procedure of Example 8 car-3-en-5-one is reacted with methylmercaptan by heating the reaction mixture in a suitable pressure-vessel for 3 hours to yield 3-methylthio-caran-5-on, boiling point ca 70° at 0.5 mm Hg, nD20 = 1.5224.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03974222 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-6055fa014a22492197fa6955f172a207 |
| Source note | uspto-grants-1976_08 |