HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23338077, compound → Methyldamascone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23338077 | HCID 23338077 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Pentane | HCID 8003 | — |
| Product | Methyldamascone | HCID 14759136 | 63% |
Reaction Steps
2,6,6-Trimethyl-1-[1-hydroxy-3-methyl-2-butenyl]-1-cyclohexene, prepared according to Example 6, (1.0 g.) with activated MnO2 (10 g.) in 30 ml. of pentane was mixed at room temperature during 63 h. After filtration and distillation 630 mg. (63 %) of the desired ketone, B.p. 67° /0.001 Torr, were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03975310 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-0e7ef268d9434eeaa3f03f61091b85b7 |
| Source note | uspto-grants-1976_08 |