1,4-Dioxane → HCID 23338024, compound

HRID 1283363Notes

Reaction equation

HRID 1283363 reaction equation
[CH3:1][C:2]1[CH2:7][CH:6](C)[CH2:5][C:4]([CH3:10])([CH3:9])[C:3]=1[C:11](=[O:16])/[C:12](/[CH3:15])=[CH:13]/[CH3:14].O1CCOC[CH2:18]1>>[CH3:1][C:2]12[C:13]([CH3:14])=[C:12]([CH3:15])[C:11](=[O:16])[CH:3]1[C:4]([CH3:10])([CH3:9])[CH:5]([CH3:18])[CH2:6][CH2:7]2

Participants

3

Reactant 2

HCID 312751,4-DioxaneHCID 23337993HCID 23337993, compound

Product 1

HCID 23338024HCID 23338024, compound

Procedure

According to the same procedure described in Example 49, a solution of 2,4,6,6-tetramethyl-1-[2-methyl-crotonoyl]-1-cyclohexene (1.0 g.) in 10 ml. of dioxan was heated at 100° under nitrogen with acidic diatomaceous earth (0.2 g.).

Sources & evidence

ORD record
ord-840e8d8185044313b9866c191f7be393
Source dataset
uspto-grants-1976_08
Patent number
US03975310

Reaction notes

Loading…