HuagongsheHuagongshe Chemistry Print Report · For research reference only
beta-Damascenone → 1,5,5,9-Tetramethylbicyclo[4.3.0]nona-2,8-dien-7-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | beta-Damascenone | HCID 5366074 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 1,5,5,9-Tetramethylbicyclo[4.3.0]nona-2,8-dien-7-one | HCID 12600925 | — |
Reaction Steps
A solution of 2,6,6-trimethyl-1-crotonoyl-1,3-cyclohexadiene (1.0 g.) in 10 ml. of dioxan was heated under the same conditions as described in Example 49 with acidic diatomaceous earth (0.2 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03975310 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-51e3fa976c414678b94f47615f4b0f02 |
| Source note | uspto-grants-1976_08 |