Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(3,5-DI-Tert-butyl-4-hydroxy-benzyl)-pentane-2,4-dione → 3-(3,5-Ditertiarybutyl-4-hydroxybenzyl)-2,4-pentanediol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(3,5-DI-Tert-butyl-4-hydroxy-benzyl)-pentane-2,4-dione | HCID 914401 | — |
| 반응물 | Aluminium lithium hydride | HCID 21226445 | — |
| 생성물 | 3-(3,5-Ditertiarybutyl-4-hydroxybenzyl)-2,4-pentanediol | HCID 20566819 | 33.2% |
반응 단계
Using the procedure of Example 1, 119 grams of 3-(3,5-ditertiarybutyl-4-hydroxybenzyl)-2,4-pentanedione was reduced with 28.2 grams of lithium aluminum hydride. There was obtained 40 grams of 3-(3,5-ditertiarybutyl-4-hydroxybenzyl)-2,4-pentanediol which melted at 102° to 105° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03975360 |
| 출처 데이터셋 | uspto-grants-1976_08 |
| ORD ID | ord-0868f48e967d43589e86e9c82fdf1159 |
| 출처 메모 | uspto-grants-1976_08 |