HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → titanium(III) trichloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Diisopentyl ether | HCID 10989 | — |
| Reactant | titanium(III) trichloride | HCID 10313229 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | titanium(III) trichloride | HCID 10313229 | — |
| Product | I2 di-isoamyl ether | HCID 131712143 | — |
Reaction Steps
Titanium trichloride composition (A) of 11.0 g was suspended in 55 ml of toluene and iodine and di-isoamyl ether were added in amounts to give a molar ratio of titanium trichloride composition (A)/I2 /di-isoamyl ether of 1.0/0.1/1.0 and then reacted at 80° C. for one hour to obtain titanium trichloride solid catalyst. This catalyst is referred to as titanium trichloride solid catalyst (II).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04259461 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-54247050930040fab4b17de526a68ef3 |
| Source note | uspto-grants-1981_03 |