Benzene → HCID 136450672, compound

Participants

Reaction Conditions

Reaction Steps

50g of 2-n-octadecylthio-5-(1-phenyl-5-tetrazolylthio)-p-benzoquinone was added to 1 liter of benzene. After adding 11g of thiophenol to this mixture, the mixture was stirred at 20°C for 6 hours. Then benzene was removed by distillation under a reduced pressure, and the resulting crystals were separated by filtration and washed with water. They were recrystallized form n-hexane. Thus 40g of needle-like crystals of 2-n-octadecylthio-5-(1-phenyl-5-tetrazolylthio)-6-phenylthiohydroquinone having a melting point of 96°C was obtained.

Provenance & Evidence