Phosgene → HCID 21453101, compound

HRID 1283436Notes

Reaction equation

HRID 1283436 reaction equation
[C:1]([Cl:4])(=[O:3])[NH2:2].[CH:5]([N:7]1[CH2:12][CH2:11][CH2:10]N[C:8]1=[O:13])=[O:6].C(Cl)(Cl)=O>>[Cl:4][C:1]([N:2]1[CH2:10][CH2:11][CH2:12][N:7]([CH:8]=[O:13])[C:5]1=[O:6])=[O:3]

Participants

4

Reactant 3

HCID 6371PhosgeneHCID 68048Carbamic chlorideHCID 21453166HCID 21453166, compound

Product 1

HCID 21453101HCID 21453101, compound

Procedure

This carbamic acid chloride was produced as described in Example 27 B from 5 parts by weight of 1-formyl-2-oxo-1,3-diaza-cyclohexane and 6 parts by weight of phosgene. The substance, an oil, was used without further purification for the production of the penicillin of Example 35 A. IR-bands at 1790, 1685, 1300 and 1165 cm-1.

Workup

  1. customThe substance, an oil, was used without further purification for the production of the penicillin of Example 35 A

Sources & evidence

ORD record
ord-3efcecd8eeee468b883791f7a3463579
Source dataset
uspto-grants-1976_08
Patent number
US03975375

Reaction notes

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