Thiomorpholine → HCID 54417899, compound

HRID 1283450Notes

Reaction equation

HRID 1283450 reaction equation
[CH3:1][S:2][C:3]1[N:8]=[C:7]([N:9]2[CH2:14][CH2:13][S:12][CH2:11][CH2:10]2)[C:6]([N+:15]([O-:17])=[O:16])=[C:5]([O:18][CH2:19][C:20](C)(C)C)[N:4]=1.ClC1C([N+]([O-])=[O:32])=C(OCC(C)(C)C)N=C(SC)N=1.N1CCSCC1>C(O)C>[CH2:19]([O:18][C:5]1[N:4]=[C:3]([S:2][CH3:1])[N:8]=[C:7]([N:9]2[CH2:14][CH2:13][S:12](=[O:32])[CH2:11][CH2:10]2)[C:6]=1[N+:15]([O-:17])=[O:16])[CH3:20]

Participants

5

Reactant 3

HCID 67164ThiomorpholineHCID 21517737HCID 21517737, compoundHCID 21517778HCID 21517778, compound

Product 1

HCID 54417899HCID 54417899, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

2-Methylthio-6-neopentoxy-5-nitro-4-thiomorpholinopyrimidine from 4-chloro-2-methylthio-6-neopentoxy-5-nitro-pyrimidine and thiomorpholine. M.p. 102°-104°C (ethanol).

Sources & evidence

ORD record
ord-5b75214f06a745839a61705382de7a74
Source dataset
uspto-grants-1976_08
Patent number
US03975384

Reaction notes

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