Benzenesulfonyl chloride → HCID 21518570, compound

HRID 1283612Notes

Reaction equation

HRID 1283612 reaction equation
[C:1]1([S:7](Cl)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:11]1[CH:15]2[CH2:16][NH:17][CH2:18][CH:14]2[CH2:13][O:12]1>N1C=CC=CC=1>[C:1]1([S:7]([N:17]2[CH2:18][CH:14]3[CH2:13][O:12][CH2:11][CH:15]3[CH2:16]2)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 7369Benzenesulfonyl chlorideHCID 21421150Hexahydro-1H-furo[3,4-c]pyrrole2×

Product 1

HCID 21518570HCID 21518570, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent2×

Conditions

Temperature
5 °C

Procedure

Benzenesulfonyl chloride (0.05 mole, 8.83 grams) dissolved in 15 ml pyridine was slowly added to a mixture of hexahydro-1H-furo(3,4-c)pyrrole, represented by formula (X), (0.05 mole, 5.66 grams) in 10 ml of pyridine at 5°C. The reaction mixture was stirred for 2 hours at 5°C. and then for 16 hours while warming to room temperature.

Workup

  1. temperaturefor 16 hours while warming to room temperature

Sources & evidence

ORD record
ord-87060387bde44ed9b1295b094e3c9c41
Source dataset
uspto-grants-1976_08
Patent number
US03975532

Reaction notes

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