Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Salicylic Acid | HCID 338 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | 2-(Dichloromethyl)phenol | HCID 18008187 | — |
Reaction Steps
A mixture of 10 grams salicylic acid, 7 ml of thionyl chloride, and 0.02 gram of aluminum chloride was heated at 40 to 45°C. for 11/2 hours. The excess thionyl chloride was removed in vacuum and the salicylyl chloride reaction product can be used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US03975532 |
|---|
| Source dataset | uspto-grants-1976_08 |
|---|
| ORD ID | ord-3e83c12fe1db40ba8056d1044542bbe6 |
|---|
| Source note | uspto-grants-1976_08 |
|---|
