HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → (2-Acetamido-3-benzoylphenyl)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Ozone | HCID 24823 | — |
| Reactant | (2-Methyl-3-phenyl-1H-indol-7-yl)acetic acid | HCID 20378312 | — |
| Product | (2-Acetamido-3-benzoylphenyl)acetic acid | HCID 15634767 | — |
Reaction Steps
A solution of 2 g. of α-(2-methyl-3-phenylindol-7-yl)acetic acid in 60 ml. of acetic acid was treated with ozone for 15 minutes. The reaction mixture was treated with 10 ml. of water and allowed to evaporate overnight. The residue (1.7 g.) was recrystallized from isopropanol; yield 1.6 g. (71%); m.p. 188°-190°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03975531 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-ebf7acb319844c61a3344a4c2244a1e1 |
| Source note | uspto-grants-1976_08 |