m-Anisoyl chloride → 2-n-Butyl-3-(3'-methoxybenzoyl)benzofuran

HRID 1283643Notes

Reaction equation

[CH2:1]([C:5]1[O:6][C:7]2[CH:13]=[CH:12][CH:11]=[CH:10][C:8]=2[CH:9]=1)[CH2:2][CH2:3][CH3:4].[C:14](Cl)(=[O:23])[C:15]1[CH:20]=[CH:19][CH:18]=[C:17]([O:21][CH3:22])[CH:16]=1>>[CH2:1]([C:5]1[O:6][C:7]2[CH:13]=[CH:12][CH:11]=[CH:10][C:8]=2[C:9]=1[C:14](=[O:23])[C:15]1[CH:20]=[CH:19][CH:18]=[C:17]([O:21][CH3:22])[CH:16]=1)[CH2:2][CH2:3][CH3:4]

Participants

Reactant 2

HCID 74374m-Anisoyl chloride

HCID 779512-Butylbenzofuran

Product 1

HCID 215186582-n-Butyl-3-(3'-methoxybenzoyl)benzofuran

Procedure

Acylation of 9.4 g. (0.054 mol.) of 2-n-butylbenzofuran with 9.9 g. (0.058 mol.) of m-anisoyl chloride according to the procedure described in Example 10 gave 2-n-butyl-3-(3'-methoxybenzoyl)benzofuran.

Sources & evidence

ORD record: ord-eedcd7a200b14d979d3d96892f955d8b
Source dataset: uspto-grants-1976_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03975537

Reaction notes

Loading…