HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → 5-Chloro-2-phenyl-3-(4-methoxybenzoyl)benzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | 5-Chloro-2-phenylbenzofuran | HCID 615042 | — |
| Product | 5-Chloro-2-phenyl-3-(4-methoxybenzoyl)benzofuran | HCID 21435398 | — |
Reaction Steps
Acylation of 5-chloro-2-phenylbenzofuran with anisoyl chloride was accomplished as described in the procedure of Example 10 to give 5-chloro-2-phenyl-3-(4'-methoxybenzoyl)benzofuran which was then demethylated and the product treated with epichlorohydrin as described above. Opening of the epoxide ring with isopropylamine as previously described gave the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03975537 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-061a0899f83f444586caf590609848ce |
| Source note | uspto-grants-1976_08 |