2,4,7-Trinitrofluoren-9-one → 2-Methyldecane

HRID 1283716Notes

Reaction equation

HRID 1283716 reaction equation
[CH:1]1[CH:6]=[C:5]2[CH:7]=[CH:8][CH:9]=[C:10]([CH2:11]CNC(CCC(O)=O)=O)[C:4]2=[CH:3][CH:2]=1.[N+](C1C=C([N+]([O-])=O)C2C3C(=CC([N+]([O-])=O)=CC=3)C(=O)C=2C=1)([O-])=O>>[CH3:3][CH2:2][CH2:1][CH2:6][CH2:5][CH2:7][CH2:8][CH2:9][CH:10]([CH3:4])[CH3:11]

Participants

3

Reactant 2

HCID 85212,4,7-Trinitrofluoren-9-oneHCID 9151746N-[2-(1-naphthyl)ethyl]succinamic acid2×

Product 1

HCID 234152-Methyldecane

Procedure

One half of the exposure zone (5.7 cm. by 5.7 cm.) of NESA glass plate 12 was coated with a 20 micron thick layer of a dark charge exchange layer 13 composed of 2,4,7-trinitro-9-fluorenone and a Butvar binder as described in the formulation given in Example 6. The other half of the NESA glass plate 12 was left uncoated.

Sources & evidence

ORD record
ord-20b5c85934414fbda743cf188af9e309
Source dataset
uspto-grants-1976_08
Patent number
US03976485

Reaction notes

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