HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → Ethyl 2-ethoxycarbonyloxyimino-2-cyanoacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Ethyl 2-cyano-2-(hydroxyimino)acetate | HCID 6399078 | — |
| Product | Ethyl 2-ethoxycarbonyloxyimino-2-cyanoacetate | HCID 54447666 | 74.3% |
Reaction Steps
The reaction of ethyl 2-hydroxyimino-2-cyanoacetate (8.5 g) with ethyl chloroformate (6.0 g) is carried out as in Example 3 to give ethyl 2-ethoxycarbonyloxyimino-2-cyanoacetate (8.8 g) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03976635 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-ea93ba963e864772abb1601bfbcdd94e |
| Source note | uspto-grants-1976_08 |