2-Nitrotoluene → HCID 12906240, compound

HRID 1283780Notes

Reaction equation

HRID 1283780 reaction equation
C(O[CH:4](OCC)[N:5]([CH3:7])[CH3:6])C.[N+:11]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1[CH3:20])([O-:13])=[O:12]>>[CH3:7][N:5]([CH3:6])/[CH:4]=[CH:20]/[C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][C:14]=1[N+:11]([O-:13])=[O:12]

Participants

3

Reactant 2

HCID 69442-NitrotolueneHCID 70913Dimethylformamide diethylacetal

Product 1

HCID 12906240HCID 12906240, compound

Procedure

A 50-ml. glass liner containing 15.6 g. of 95% dimethylformamide diethyl acetal and 13.7 g. of o-nitrotoluene was pressurized with nitrogen in an autoclave to 35 atm. and then heated to 155° for 24 hours.

Workup

  1. additionglass liner containing 15.6 g
  2. temperatureheated to 155° for 24 hours

Sources & evidence

ORD record
ord-c11ea1b05c55464f8086adfbbfeeab8c
Source dataset
uspto-grants-1976_08
Patent number
US03976639

Reaction notes

Loading…