HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propyl isocyanate → 3-(N-propylcarbamoyl)-1,3-bis(2-cyano-5-trifluoromethylphenyl)triazene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propyl isocyanate | HCID 61033 | — |
| Reactant | 1,3-Bis(2-cyano-5-(trifluoromethyl)phenyl)triazene | HCID 3035495 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 3-(N-propylcarbamoyl)-1,3-bis(2-cyano-5-trifluoromethylphenyl)triazene | HCID 21516389 | — |
Reaction Steps
To a solution of 5.4 g. (0.014 mol.) of 1,3-bis(2cyano-5-trifluoromethylphenyl)triazene in 500 ml. of ether is added 15 ml. of propyl isocyanate. The reaction mixture is stirred at 25° for 24 hours after which time the precipitated product is collected by filtration and washed with ether to give 3-(N-propylcarbamoyl)-1,3-bis(2-cyano-5-trifluoromethylphenyl)triazene, m.p. 138°-140° (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03976633 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-a99a80ced4654726bee9ded7d91fff25 |
| Source note | uspto-grants-1976_08 |