HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylamine → HCID 13336929, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylamine | HCID 7852 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 12907203 | HCID 12907203 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13336929 | HCID 13336929 | 85.5% |
Reaction Steps
2,3-Dicyano-5-chloro-6-isobutylpyrazine (1.10 g; 0.005 mole) was dissolved in 20 ml of tetrahydrofuran. The solution was worked up in the same way as in Example 13 using 0.30 g (0.005 mole) of n-propylamine and 0.02 g (0.005 mole) of sodium hydroxide to afford 1.04 g (yield 85%) of 2,3-dicyano-5-n-propylamino-6-isobutylpyrazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04259489 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-386cffca1c424e9da23ddfe66cb872ac |
| Source note | uspto-grants-1981_03 |