HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Isothiocyanate → HCID 12898123, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Isothiocyanate | HCID 2346 | — |
| Reactant | 2-Imidazolidinone | HCID 8453 | — |
| Reactant | 1H-Imidazole-2-carbothioamide | HCID 18521648 | — |
| Product | HCID 12898123 | HCID 12898123 | — |
Reaction Steps
The starting thiocarbamoylimidazole required for the above reaction is made as follows: 86g ethyleneurea and 149g benzylisothiocyanate are treated together with stirring for 6 hrs. at 150°. Upon cooling, a solid mass is obtained, which is triturated with ether and then with hot alcohol and filtered. Recrystallization from chloroform-methanol gives 1-(benzylthiocarbamoyl)-2-oxo-tetrahydroimidazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03976778 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-45316cad97fb4fdba63b175ddcfdecf4 |
| Source note | uspto-grants-1976_08 |