HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl Isothiocyanate → 4-Cyclohexyl 2-phenylthiocarbamoyl cyclohexanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl Isothiocyanate | HCID 7673 | — |
| Reactant | 4-Cyclohexyl 1-morpholyl cyclohex-1 ene | HCID 21515286 | — |
| Reactant | 4-Cyclohexyl 2-phenylthiocarbamoyl 1-morpholyl cyclohex-1 ene | HCID 21515287 | — |
| Product | 4-Cyclohexyl 2-phenylthiocarbamoyl cyclohexanone | HCID 21515296 | — |
Reaction Steps
Using the procedure of example 1 and starting from 9.2 g of 4-cyclohexyl 1-morpholyl cyclohex-1 ene and from 5 g phenyl isothiocyanate 7.8 g of 4-cyclohexyl 2-phenylthiocarbamoyl 1-morpholyl cyclohex-1 ene are obtained, melting at 143°. Acid hydrolysis of 7 g of 4-cyclohexyl 2-phenylthiocarbamoyl 1-morpholyl cyclohex- 1 ene gives 4.5 g of 4-cyclohexyl 2-phenylthiocarbamoyl cyclohexanone which melts at 150° .
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03978044 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-914beedd92da42558ef712283be20d67 |
| Source note | uspto-grants-1976_08 |