HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 152749587, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | HCID 178473545 | HCID 178473545 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 152749587 | HCID 152749587 | — |
Reaction Steps
5.1 parts by weight of methylisocyanate were added to a suspension of 10 parts by weight of ethoxycarbonylguanidine (manufactured according to Isr. J. Chem. 8, 651 [1970] ) in 60 parts by volume of anhydrous dioxane, in the course of which the temperature rose to 45°C and the precipitate dissolved. After a short time, a crystalline precipitate separated out again, which was filtered off after cooling and washed with ether. It was dried in vacuo over P2O5 and paraffin chips.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03978056 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-57820e630b364996b0cf8005bfb08923 |
| Source note | uspto-grants-1976_08 |