Methanol → Methyl 2-oxoimidazolidine-1-carboxylate

Participants

Reaction Steps

14.9 parts by weight of N-chlorocarbonyl-imidazolid-2-one were introduced into 70 parts by volume of ice-cold methanol and the mixture was stirred for 1 hour at room temperature and subsequently for 1 hour at 40°-50° C. After stripping off the excess methanol, the product was recrystallized from acetone.

Provenance & Evidence