HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-[3-(N-Benzyl-N-ethylamino)-propyl]-5H-dibenzo[a,d]cycloheptene → 5-(3-ethylaminopropyl)-5H-dibenzo[a,d]cycloheptene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-[3-(N-Benzyl-N-ethylamino)-propyl]-5H-dibenzo[a,d]cycloheptene | HCID 21412139 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 5-(3-ethylaminopropyl)-5H-dibenzo[a,d]cycloheptene | HCID 21412102 | — |
Reaction Steps
5-[3-(N-Benzyl-N-ethylamino)-propyl]-5H-dibenzo[a,d]cycloheptene is dissolved in absolute alcohol and hydrogenated over palladium on alumina catalyst at 40°-60°C. The catalyst is separated and the product isolated by evaporating the solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03978121 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-e7e3bc02e0d34ec4bf6617f946b934dd |
| Source note | uspto-grants-1976_08 |